6-[(苯基甲氧基)甲基]-1,4-二恶烷-2-甲醇合成路线 （共 6 条）
反应条件
hydrogenchloride in methanol
T=20°C;
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
hydrogenchloride in methanol
T=20°C;
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
1: 88 percent / NaH / 4 h / 20 °C
2: 8 percent / I2; NaHCO3 / H2O; diethyl ether / 3 h / 0 °C
3: 63 percent / 18-crown-6 / dimethylformamide / 24 h / 80 °C
4: 90 percent / HCl / methanol / 20 °C
View Scheme
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
1: 8 percent / I2; NaHCO3 / H2O; diethyl ether / 3 h / 0 °C
2: 63 percent / 18-crown-6 / dimethylformamide / 24 h / 80 °C
3: 90 percent / HCl / methanol / 20 °C
View Scheme
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
1: 63 percent / 18-crown-6 / dimethylformamide / 24 h / 80 °C
2: 90 percent / HCl / methanol / 20 °C
View Scheme
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
反应条件
1: 88 percent / NaH / 4 h / 20 °C
2: 8 percent / I2; NaHCO3 / H2O; diethyl ether / 3 h / 0 °C
3: 63 percent / 18-crown-6 / dimethylformamide / 24 h / 80 °C
4: 90 percent / HCl / methanol / 20 °C
View Scheme
参考文献
Cassel, Stephanie; Debaig, Catherine; Benvegnu, Thierry; Chaimbault, Patrick; Lafosse, Michel; Plusquellec, Daniel; Rollin, Patrick
European Journal of Organic Chemistry, 2001 , # 5 p. 875 - 896
