2,3,5,6-四氟-4-甲基苯甲醇合成路线 (共 5 条)
反应条件
hydrogen; magnesium oxide; palladium on activated carbon in methanol; water T=50°C; P=1875.19 Torr; 1 - 1.5 h; Product distribution / selectivity;
参考文献
Jiangsu Yangnong Chemical Co., Ltd.
Patent: US2007/55075 A1, 2007 ;
Location in patent: Page/Page column 4 ;
反应条件
hydrogen; sponge cobalt catalyst in water-containing state in toluene T=160°C; P=3975.4 - 165017 Torr; 0.5 - 1 h; Product distribution / selectivity;
参考文献
US2004/10167 A1, ;
Page 3-5 ;
反应条件
hydrogen; cobalt R400 in toluene T=120 - 150°C; P=3750.38 - 5625.56 Torr; 10.5 h; Autoclave; Product distribution / selectivity;
参考文献
US2010/145106 A1, ;
Page/Page column 5 ;
反应条件
hydrogen; 5-palladium/activated carbon in water; butan-1-ol T=100°C; 16 h; Inert atmosphere; Product distribution / selectivity;
参考文献
EP2123624 A1, ;
Page/Page column 13 ;
反应条件
toluene-4-sulfonic acid in ethanol 0.5 h; Reflux;
参考文献
Journal of Fluorine Chemistry, , vol. 130, # 10 p. 938 - 941