4-(3,4-二氯苯基)-1-四氢萘酮合成路线 （共 39 条）
反应条件
oxygen; sodium hydride in tetrahydrofuran T=0 - 20°C; 5 h;
参考文献
Wang, Xinbo; Wang, David Zhigang
Tetrahedron, 2011 , vol. 67, # 19 p. 3406 - 3411
反应条件
AlCl3, aluminium chloride T=100°C; 1.5 h; Inert atmosphere;
参考文献
Lee, Sang Hwi; Kim, In Su; Li, Qing Ri; Dong, Guang Ri; Jeong, Lak Shin; Jung, Young Hoon
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 10011 - 10019
反应条件
hydrogen; SA-3135 support, Co(NO3)2, H2O; dried and calcined ones or twice (Co 11 - 25percent); reduction with H2 in tetrahydrofuran T=120 - 150°C; P=6000.6 Torr;
参考文献
WO2004/92110 A2, ;
Page 19-22 ;
反应条件
boron trifluoride diethyl etherate; trifluoroacetic anhydride in dichloromethane T=40 - 45°C; 5 h; Product distribution / selectivity;
参考文献
UNICHEM LABORATORIES LIMITED
Patent: WO2007/119247 A2, 2007 ;
Location in patent: Page/Page column 22 ;
反应条件
aluminum tri-bromide in methanol; water; 1,2-dichloro-benzene
参考文献
Delalande S.A.
Patent: US5019655 A1, 1991 ;
反应条件
aluminium chloride in water; 1,2-dichloro-benzene
参考文献
Delalande S.A.
Patent: US5019655 A1, 1991 ;
反应条件
AlCl3, aluminium chloride T=100°C; 4 h; Inert atmosphere;
参考文献
Chen, Fei; Ding, Ziyuan; He, Yanmei; Qin, Jie; Wang, Tianli; Fan, Qing-Hua
Tetrahedron, 2012 , vol. 68, # 26 p. 5248 - 5257
反应条件
sodium hydroxide; trifluorormethanesulfonic acid in hexane; dichloromethane; benzene
反应条件
sodium hydroxide in hexane; dichloromethane; water; polypropylene; benzene
反应条件
1: potassium tert-butoxide / 2-methyl-propan-2-ol / 16 h / Heating 2: 50 percent / 48percent aq. HBr / acetic acid / 36 h / Heating 3: 100 percent / H2 / 5percent Pd/C / ethyl acetate / 24 h / 760 Torr / Ambient temperature 4: SOCl2 / toluene / 1.25 h 5: AlCl3 / CS2 / 16 h / Ambient temperature View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 27, # 11 p. 1508 - 1515
