3,3-二甲基-2-亚甲基丁酸甲酯合成路线 （共 7 条）
反应条件
in benzene-d6 T=24°C; Irradiation;
参考文献
Griesser, Markus; Neshchadin, Dmytro; Dietliker, Kurt; Moszner, Norbert; Liska, Robert; Gescheidt, Georg
Angewandte Chemie - International Edition, 2009 , vol. 48, # 49 p. 9359 - 9361
反应条件
methanol; Pd-BaSO4 Hydrogenation;
参考文献
Crawford; Swift
Journal of the Chemical Society, 1952 , p. 1220,1222
反应条件
1-methyl-pyrrolidin-2-one; palladium diacetate; methanesulfonic acid; Ph2Ppym
T=60°C; P=45003.6 Torr; 2 h;
参考文献
Reetz, Manfred T.; Demuth, Ralf; Goddard, Richard
Tetrahedron Letters, 1998 , vol. 39, # 39 p. 7089 - 7092
反应条件
copper(I) bromide dimethylsulfide complex; zinc(II) chloride in tetrahydrofuran; diethyl ether
-70 deg C, 1 h; 0 deg C, overnight;
参考文献
Xu, Long-He; Kuendig, Ernst Peter
Helvetica Chimica Acta, 1994 , vol. 77, # 6 p. 1480 - 1484
反应条件
1: 94 percent / N-chlorosuccinimide, Me2S / CH2Cl2 / 20 h / 0 °C
2: 86 percent / CuBr*Me2S, ZnCl2 / tetrahydrofuran; diethyl ether / -70 deg C, 1 h; 0 deg C, overnight
View Scheme
参考文献
Xu, Long-He; Kuendig, Ernst Peter
Helvetica Chimica Acta, 1994 , vol. 77, # 6 p. 1480 - 1484
反应条件
1: aqueous dimethylamine; water
2: sulfuric acid
View Scheme
参考文献
Crawford
Journal of the Chemical Society, 1953 , p. 2658,2659
参考文献
Crawford
Journal of the Chemical Society, 1953 , p. 2658,2659
