1: 91 percent / TFA / 1 h / Heating
2: 91 percent / m-chloroperbenzoic acid, sodium carbonate / CH2Cl2 / 72 h / Ambient temperature
3: 89 percent / BuLi / tetrahydrofuran / 1 h / Ambient temperature
4: 79 percent / NaH / tetrahydrofuran / 1.) 0 deg C, 0.5 h, 2.) reflux, 2 h
5: 72 h / Irradiation
View Scheme
参考文献
Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1169 - 1172
1: 91 percent / m-chloroperbenzoic acid, sodium carbonate / CH2Cl2 / 72 h / Ambient temperature
2: 89 percent / BuLi / tetrahydrofuran / 1 h / Ambient temperature
3: 79 percent / NaH / tetrahydrofuran / 1.) 0 deg C, 0.5 h, 2.) reflux, 2 h
4: 72 h / Irradiation
View Scheme
参考文献
Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1169 - 1172
1: 89 percent / BuLi / tetrahydrofuran / 1 h / Ambient temperature
2: 79 percent / NaH / tetrahydrofuran / 1.) 0 deg C, 0.5 h, 2.) reflux, 2 h
3: 72 h / Irradiation
View Scheme
参考文献
Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1169 - 1172
1: 90 percent / LiAlH4 / diethyl ether / 0.5 h / 0 °C
2: 97.5 percent / toluene-p-sulphonic acid / benzene / 0.25 h / Heating
View Scheme
参考文献
Hannaby, Malcolm; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 303 - 311
Torr, Richard S.; Warren, Stuart
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 1169 - 1172
