N-二异丙基-4-溴苯甲酰胺合成路线 （共 7 条）
反应条件
triethylamine in tetrahydrofuran T=0°C;
参考文献
WO2008/112217 A1, ;
Page/Page column 78 ;
WO 2008/112217 A1
反应条件
4-(N,N-dimethlyamino)pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride in dichloromethane 6 h; Heating;
参考文献
Furayama, Taniyuki; Yonehara, Mitsuhiro; Arimoto, Sho; Kobayashi, Minoru; Matsumoto, Yotaro; Uchiyama, Masanobu
Chemistry - A European Journal, 2008 , vol. 14, # 33 p. 10348 - 10356
反应条件
in dichloromethane Substitution; 0.25 h;
参考文献
Archiv der Pharmazie, , vol. 333, # 5 p. 145 - 153
反应条件
1: thionyl chloride; N,N-dimethyl-formamide / toluene / 20 °C 2: triethylamine / dichloromethane / 0 - 20 °C View Scheme
参考文献
Organic Letters, , vol. 16, # 2 p. 390 - 393
反应条件
1: tri-isopropoxy-borane; para-bromobenzonitrile; lithium diisopropyl amide 2: 3-hydroxy-2,2-dimethylpropanol Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 71, # 6 p. 2518 - 2520
反应条件
hydrogenchloride; zinc(II) chloride T=160°C; 72 h;
参考文献
European Journal of Organic Chemistry, , # 8 p. 1689 - 1696
反应条件
zirconocene dichloride; lithium tri-t-butoxyaluminum hydride in tetrahydrofuran T=20°C; 0.416667 h;
参考文献
Zhao, Yigang; Snieckus, Victor
Organic Letters, 2014 , vol. 16, # 2 p. 390 - 393
