反应条件
1.1: 82 percent / p-toluenesulfonic acid / toluene / 5 h / Heating
2.1: 95 percent / Pd(OAc)2; [Bu4N]Br; KOAc / dimethylformamide / 24 h / Heating
3.1: 92 percent / aq. HCl / tetrahydrofuran / 5 h / Heating
4.1: BH3*THF / tetrahydrofuran / 3 h / 20 °C
4.2: NaCNBH3; AcOH / 3 h / 20 °C
4.3: 75 percent / aq. NaOH; KMnO4 / CH2Cl2 / 2 h / 20 °C
View Scheme
参考文献
De, Subhadip; Ghosh, Santanu; Bhunia, Subhajit; Sheikh, Javeed Ahmad; Bisai, Alakesh
Organic Letters, 2012 , vol. 14, # 17 p. 4466 - 4469
