反应条件
1.1: 95 percent / p-toluenesulfonic acid / toluene / 5 h / Heating
2.1: 95 percent / Pd(OAc)2; [Bu4N]Br; KOAc / dimethylformamide / 5 h / Heating
3.1: 92 percent / aq. HCl / tetrahydrofuran / 5 h / Heating
4.1: BH3*THF / tetrahydrofuran / 3 h / 20 °C
4.2: NaCNBH3; AcOH / 3 h / 20 °C
4.3: 75 percent / aq. NaOH; KMnO4 / CH2Cl2 / 2 h / 20 °C
View Scheme
参考文献
Torres, Jose C.; Pinto, Angelo C.; Garden, Simon J.
Tetrahedron, 2004 , vol. 60, # 44 p. 9889 - 9900
