反应条件
1.1: sec.-butyllithium / diethyl ether; hexane; cyclohexane / 1 h / -78 °C / Inert atmosphere 1.2: 2 h / -78 °C / Inert atmosphere 2.1: cesium fluoride / dichloromethane; water / 16 h / 20 °C 3.1: tetrahydrofuran / 2 h / 20 °C 4.1: dihydrogen peroxide; sodium hydroxide / water / 0 - 20 °C 5.1: Jone's reagent / acetone / 0 - 20 °C 6.1: chlorosulfonic acid / dichloromethane / 0.75 h / 20 °C 7.1: sodium acetate / ethanol / 15 h / Reflux 7.2: 20 h / 20 °C / 760.05 Torr View Scheme
参考文献
Organic Letters, , vol. 13, # 21 p. 5740 - 5743
