N-[(2S)-1-氧代-1-(苯基甲氧基氨基)丙-2-基]氨基甲酸叔丁酯合成路线 (共 4 条)
反应条件
benzotriazol-1-ol; triethylamine; dicyclohexyl-carbodiimide in dichloromethane; N,N-dimethyl-formamide
T=5°C;
参考文献
Odake; Okayama; Obata; Morikawa; Hattori; Hori; Nagai
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 4 p. 1007 - 1011
反应条件
phosphoric acid di-Et ester 2-phenylbenzimidazol-1-yl ester in N,N-dimethyl-formamide
T=20°C;
参考文献
Kokare, Nagnnath D.; Nagawade, Rahul R.; Rane, Vipul P.; Shinde, Devanand B.
Tetrahedron Letters, 2007 , vol. 48, # 25 p. 4437 - 4440
反应条件
lithium hexamethyldisilazane in tetrahydrofuran
T=-78°C;
参考文献
Gissot, Arnaud; Volonterio, Alessandro; Zanda, Matteo
Journal of Organic Chemistry, 2005 , vol. 70, # 17 p. 6925 - 6928
反应条件
N-[(diphenylphosphoryl)oxy]-2-phenyl-1H-benzimidazole
Title compound not separated from byproducts.;
参考文献
Kokare, Nagnnath D.; Shinde, Devanand B.
Journal of Heterocyclic Chemistry, 2008 , vol. 45, # 4 p. 981 - 986