2-脱氧-2-N-邻苯二甲酰亚胺基-1,3,4,6-四-O-乙酰基-D-吡喃葡萄糖合成路线 （共 5 条）
反应条件
With dichloromethoxy methane; boron trifluoride diethyl etherate in chloroform T=65°C; 3 h; Inert atmosphere; Show Experimental Procedure
参考文献
Bednarczyk, Dorota; Walczewska, Agata; Grzywacz, Daria; Sikorski, Artur; Liberek, Beata; Myszka, Henryk Carbohydrate Research, 2013 , vol. 367, p. 10 - 17
反应条件
Multi-step reaction with 2 steps 1.1: boron trifluoride diethyl etherate / dichloromethane / 24 h / 20 °C / |Inert atmosphere2.1: sodium methylate / methanol / -10 °C / |Inert atmosphere2.2: Amberlite ion exchange resin / pH 7
参考文献
Wasonga, Gilbert; Tatara, Yota; Kakizaki, Ikuko; Huang, Xuefei Journal of Carbohydrate Chemistry, 2013 , vol. 32, # 5-6 p. 392 - 409
反应条件
Multi-step reaction with 3 steps 1.1: boron trifluoride diethyl etherate / dichloromethane / 24 h / 20 °C / |Inert atmosphere2.1: sodium methylate / methanol / -10 °C / |Inert atmosphere2.2: Amberlite ion exchange resin / pH 73.1: camphor-10-sulfonic acid / acetonitrile / 3 h / |Inert atmosphere
参考文献
Wasonga, Gilbert; Tatara, Yota; Kakizaki, Ikuko; Huang, Xuefei Journal of Carbohydrate Chemistry, 2013 , vol. 32, # 5-6 p. 392 - 409
反应条件
With trimethylsilylazide; tin(IV) chloride in dichloromethane 24 h; Ambient temperature;
参考文献
Szilagyi, Laszlo; Gyoergydeak, Zoltan Carbohydrate Research, 1985 , vol. 143, p. 21 - 42
反应条件
Multi-step reaction with 2 steps 1: 76 percent / TMSOTf / CH2Cl2 / 7 h / 20 °C2: NaOMe / methanol; CH2Cl2 / 2 h / -10 °C
参考文献
Hernandez-Torres, Jesus M.; Liew, Siong-Tern; Achkar, Jihane; Wei, Alexander Synthesis, 2002 , # 4 p. 487 - 490
