2-乙基-1-甲氧基-4-甲基苯合成路线 （共 10 条）
参考文献
v. Auwers; Mauss
Chemische Berichte, 1928 , vol. 61, p. 1502
反应条件
n-butyllithium; hexane; potassium tert-butylate
1) heptane, room temperature, 2 h, 2) THF; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bates, Robert B.; Siahaan, Teruna J.; Suvannachut, Kessara
Journal of Organic Chemistry, 1990 , vol. 55, # 4 p. 1328 - 1334
反应条件
n-butyllithium; potassium tert-butylate
1.) heptane, hexane, reflux, 18 h, 2.) THF, 0 deg C, 18 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Bates, Robert B.; Siahaan, Teruna J.; Suvannachut, Kessara; Vasey, Stephen K.; Yager, Kraig M.
Journal of Organic Chemistry, 1987 , vol. 52, # 20 p. 4605 - 4608
反应条件
n-butyllithium; potassium tert-butylate
1.) heptane, hexane, reflux, 18 h, 2.) THF, 0 deg C, 18 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Bates, Robert B.; Siahaan, Teruna J.; Suvannachut, Kessara; Vasey, Stephen K.; Yager, Kraig M.
Journal of Organic Chemistry, 1987 , vol. 52, # 20 p. 4605 - 4608
反应条件
n-butyllithium; potassium tert-butylate
1.) heptane, hexane, reflux, 18 h, 2.) THF, 0 deg C, 18 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Bates, Robert B.; Siahaan, Teruna J.; Suvannachut, Kessara; Vasey, Stephen K.; Yager, Kraig M.
Journal of Organic Chemistry, 1987 , vol. 52, # 20 p. 4605 - 4608
反应条件
1: titanium tetrachloride
2: amalgamated zinc, HCl
View Scheme
参考文献
Fischer, Alfred; Henderson, George N.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2314 - 2327
反应条件
1: amalgamated zinc, HCl
View Scheme
参考文献
Fischer, Alfred; Henderson, George N.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2314 - 2327
反应条件
in water-d2
T=35°C; Product distribution;
参考文献
Fischer, Alfred; Henderson, George N.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2314 - 2327
反应条件
hexadeuterioacetone; sulfuric acid
T=35°C; Product distribution;
参考文献
Fischer, Alfred; Henderson, George N.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 2314 - 2327
反应条件
boron tribromide in dichloromethane
T=0°C; 1 h;
参考文献
JUBILANT BIOSYS LTD.; SARMA, Pakala Kumara Savithru; ACHARYA, Vinod Parameshwaran; KASIBHATLA, Srinivas Rao; VISWANADHAN, Vellarkad Narayana; TIWARI, Atul; SINGHA, Rakesh Kumar; BISCHOFF, Alexander
Patent: WO2012/90219 A2, 2012 ;
Location in patent: Page/Page column 87 ;
