6-羟基-2,2’,4,4’-四溴联苯醚合成路线 （共 4 条）
反应条件
bromine; tert-butylamine in dichloromethane; toluene T=-70 - -60°C; 4 h;
参考文献
Marsh, Goeran; Stenutz, Roland; Bergman, Ake
European Journal of Organic Chemistry, 2003 , # 14 p. 2566 - 2576
反应条件
sodium hydroxide; tetra(n-butyl)ammonium hydroxide in dichloromethane; water T=20°C; 5 h;
参考文献
Marsh, Goeran; Stenutz, Roland; Bergman, Ake
European Journal of Organic Chemistry, 2003 , # 14 p. 2566 - 2576
反应条件
boron tribromide in dichloromethane
T=50°C;
参考文献
Marsh, Goeran; Stenutz, Roland; Bergman, Ake
European Journal of Organic Chemistry, 2003 , # 14 p. 2566 - 2576
反应条件
1: K2CO3 / acetone / 12 h / 80 °C
2: H2 / 10percent Pd-C / methanol / 25 °C
View Scheme
参考文献
Carte, Brad; Faulkner, D. John
Tetrahedron, 1981 , vol. 37, p. 2335 - 2340
