反应条件
1: 98.4 percent / NaHCO3, N-bromosuccinimide / tetrahydrofuran / 2 h / -78 °C
2: 33.3 g / MCPBA, NaHCO3 / CH2Cl2; H2O / 20 °C
3: periodic acid / tetrahydrofuran; H2O / 0.15 h / 22 °C
View Scheme
参考文献
Hajos, Zoltan G.; Wachter, Michael P.; Werblood, Harvey M.; Adams, Richard E.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2600 - 2608
