反应条件
1.1: sec.-butyllithium; N,N,N',N,-tetramethylethylenediamine / diethyl ether; cyclohexane; hexane / 4 h / -78 °C
1.2: 1.17 h
1.3: |Reflux
2.1: silver(l) oxide; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) / ethylene glycol dimethyl ether / 18 h / 90 °C / |Glovebox
View Scheme
参考文献
Chausset-Boissarie, Laetitia; Ghozati, Kazem; Labine, Emily; Chen, Jack L.-Y.; Aggarwal, Varinder K.; Crudden, Cathleen M.
Chemistry - A European Journal, 2013 , vol. 19, # 52 p. 17698 - 17701
