S-(-)-吲哚啉-2-羧酸合成路线 （共 38 条）
反应条件
1.1: oxygen; potassium carbonate / water / 5 h / 120 °C / 3000.3 Torr / |Autoclave 2.1: 5 palladium on charcoal; hydrogen / water / 4 h / 60 °C / 3750.38 Torr / |Autoclave 3.1: hydrogenchloride / water / 0.5 h / 0 °C 3.2: 1 h 3.3: 3 h / 55 °C View Scheme
参考文献
Research on Chemical Intermediates, , vol. 39, # 3 p. 1143 - 1152
反应条件
1.1: nitric acid; sulfuric acid / 3 h / 0 °C 2.1: sulfuric acid; urea hydronitrate / 5 h / 0 - 60 °C 3.1: oxygen; potassium carbonate / water / 5 h / 120 °C / 3000.3 Torr / |Autoclave 4.1: 5 palladium on charcoal; hydrogen / water / 4 h / 60 °C / 3750.38 Torr / |Autoclave 5.1: hydrogenchloride / water / 0.5 h / 0 °C 5.2: 1 h 5.3: 3 h / 55 °C View Scheme
参考文献
Research on Chemical Intermediates, , vol. 39, # 3 p. 1143 - 1152
参考文献
Agricultural and Biological Chemistry, , vol. 51, # 7 p. 1833 - 1838
反应条件
1: 43 percent 2: aq. 2N HCl View Scheme
参考文献
Agricultural and Biological Chemistry, , vol. 51, # 7 p. 1833 - 1838
反应条件
hydrogen; acetic acid; platinum(IV) oxide T=60°C; 24 h; atmospheric pressure;
参考文献
Sayago, Francisco J.; Pueyo, Maria J.; Calaza, M. Isabel; Jimenez, Ana I.; Cativiela, Carlos
Chirality, 2011 , vol. 23, # 7 p. 507 - 513
反应条件
1: 66 percent / H2 / 10percent Pd/C / acetic acid / 18 h / 50 °C / 36775.4 Torr 2: 93 percent / toluene / 4 h / Heating View Scheme
参考文献
Pascard; Guilhem; Vincent; Remond; Portevin; Laubie
Journal of Medicinal Chemistry, 1991 , vol. 34, # 2 p. 663 - 669
反应条件
1: SOCl2 2: hydrogen / Pd/C / ethanol View Scheme
参考文献
Vincent; Remond; Portevin; et al.
Tetrahedron Letters, 1982 , vol. 23, # 16 p. 1677 - 1680
反应条件
rhodium in 1,4-dioxane; methanol; water
参考文献
Adir Et Cie
Patent: US4914214 A1, 1990 ;
反应条件
hydrogen; acetic acid; platinum(IV) oxide T=60°C; 24 h; atmospheric pressure;
参考文献
Sayago, Francisco J.; Pueyo, Maria J.; Calaza, M. Isabel; Jimenez, Ana I.; Cativiela, Carlos
Chirality, 2011 , vol. 23, # 7 p. 507 - 513
参考文献
Tetrahedron Letters, , vol. 34, # 38 p. 6063 - 6066
