2-甲基-2-丙基(1-氧代-1-苯基-2-丙基)氨基甲酸酯合成路线 （共 11 条）
反应条件
isopropylmagnesium chloride in tetrahydrofuran
T=-15 - 20°C;
参考文献
Liu, Jinchu; Ikemoto, Norihiro; Petrillo, Daniel; Armstrong III, Joseph D.
Tetrahedron Letters, 2002 , vol. 43, # 46 p. 8223 - 8226
反应条件
pyridinium chlorochromate in dichloromethane
1.5 h; Ambient temperature;
参考文献
Besse; Veschambre; Dickman; Chenevert
Journal of Organic Chemistry, 1994 , vol. 59, # 26 p. 8288 - 8291
反应条件
pyridinium chlorochromate in dichloromethane
1.5 h; Ambient temperature;
参考文献
Hwang, Gweon Il; Chung, Jae-Ho; Lee, Won Koo
Tetrahedron, 1996 , vol. 52, # 37 p. 12111 - 12116
反应条件
1: H2 / 10percent Pd/C / ethyl acetate / 24 h / Ambient temperature
2: 86 percent / PCC / CH2Cl2 / 1.5 h / Ambient temperature
View Scheme
参考文献
Besse; Veschambre; Dickman; Chenevert
Journal of Organic Chemistry, 1994 , vol. 59, # 26 p. 8288 - 8291
参考文献
Buckley, Thomas F.; Rapoport, Henry
Journal of the American Chemical Society, 1981 , vol. 103, # 20 p. 6157 - 6163
反应条件
in diethyl ether
T=-78°C; 4 h;
参考文献
Wolf; Pfander
Helvetica Chimica Acta, 1986 , vol. 69, # 6 p. 1498 - 1504
反应条件
in tetrahydrofuran
4 h;
参考文献
Zhou, Zheng Hong; Tang, Yi Long; Li, Kang Ying; Liu, Bing; Tang, Chu Chi
Heteroatom Chemistry, 2003 , vol. 14, # 7 p. 603 - 606
反应条件
1: 94.3 percent / N,N'-dicyclohexylcarbodiimide / CHCl3
2: 47.5 percent / tetrahydrofuran / 4 h
View Scheme
参考文献
Zhou, Zheng Hong; Tang, Yi Long; Li, Kang Ying; Liu, Bing; Tang, Chu Chi
Heteroatom Chemistry, 2003 , vol. 14, # 7 p. 603 - 606
反应条件
1: triethylamine / dichloromethane / 0 - 20 °C
2: Dess-Martin periodane / dichloromethane; water / 0.33 h / 20 °C
View Scheme
参考文献
Steves, Janelle E.; Stahl, Shannon S.
Journal of the American Chemical Society, 2013 , vol. 135, # 42 p. 15742 - 15745
反应条件
trifluoroacetic acid in dichloromethane
0.333333 h;
参考文献
Wolf; Pfander
Helvetica Chimica Acta, 1986 , vol. 69, # 6 p. 1498 - 1504
