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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
79841-55-7
合成路线
(共 6 条)
79841-55-7
→
反应条件
58-72-0
三苯乙烯
反应条件
2: 60 percent / Et4NF View Scheme
参考文献
Barbaro, Gaetano; Battaglia, Arturo; Giorgianni, Patrizia; Maccagnani, Gaetano; Macciantelli, Dante; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 381 - 386
79841-55-7
→
反应条件
13187-62-7
反应条件
1: 55 percent 2: Et4NF View Scheme
参考文献
Bonini, Bianca F.; Maccagnani, Gaetano; Mazzanti, Germana; Abdel-lateef, Ghamel; Atwa, Achmed; et al.
Heterocycles, 1990 , vol. 31, # 1 p. 47 - 57
79841-55-7
→
反应条件
115691-17-3
反应条件
1: 79 percent / diethyl ether 2: 97 percent / 1 M tetrabutylammonium fluoride (TBAF) / tetrahydrofuran; H2O / 12 h / Ambient temperature 3: 97 percent / m-chloroperbenzoic acid / CHCl3 / 2 h / Ambient temperature View Scheme
参考文献
Bonini, Bianca F.; Lenzi, Alberto; Maccagnani, Gaetano; Barbaro, Gaetano; Giorgianni, Patrizia; Macciantelly, Dante
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 2643 - 2646
79841-55-7
+
908093-98-1
→
反应条件
79841-58-0
反应条件
in diethyl ether Ambient temperature;
参考文献
Barbaro, Gaetano; Battaglia, Arturo; Giorgianni, Patrizia; Maccagnani, Gaetano; Macciantelli, Dante; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 381 - 386
1221-72-3
+
79841-55-7
→
反应条件
79841-59-1
反应条件
in diethyl ether Ambient temperature;
参考文献
Barbaro, Gaetano; Battaglia, Arturo; Giorgianni, Patrizia; Maccagnani, Gaetano; Macciantelli, Dante; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 381 - 386
79841-55-7
→
反应条件
531-05-5
2,4,6-三苯基-1,3,5-三硫杂环己烷
反应条件
1: 18.6 percent / hydrogen chloride, hydrogen sulphide / diethyl ether / 0 °C 2: 70.6 percent / tetrabutylammonium fluoride / tetrahydrofuran; H2O / 0.25 h / 0 °C View Scheme
参考文献
Bonini, Bianca F.; Mazzanti, Germana; Zani, Paolo; Maccagnani, Gaetano
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 1499 - 1502