反应条件
1: 2-(trimethylsilyl)-1,3-dithiane With cyclohexane; sec.-butyllithium in tetrahydrofuran; hexane
T=-70 - 0°C; Inert atmosphere;
2: 4-ketocyclohexanecarboxylic acid ethyl ester in tetrahydrofuran; hexane
T=-70 - 20°C; 6 h; Inert atmosphere;
参考文献
JNC Corporation; JNC Petrochemical Corporation; MASUKAWA, Tokifumi
Patent: EP2690103 A1, 2014 ;
Location in patent: Paragraph 0333 ;