1: 11-bromo-undecanoic acid With 1-hydroxy-pyrrolidine-2,5-dione; dicyclohexyl-carbodiimide in dichloromethane
T=25°C; 2 h;
2: 1-dodecylamine With 4-(N,N-dimethlyamino)pyridine in dichloromethane
T=35°C; 2 h; Further stages.;
参考文献
Battaggia, Simone; Smith, Emma E.; Vyle, Joseph S.
Nucleosides, Nucleotides and Nucleic Acids, 2007 , vol. 26, # 3 p. 245 - 254
1: SOCl2 / CH2Cl2 / 2 h / Heating
2: 2.4 g / Et3N / CH2Cl2 / 12 h / Heating
View Scheme
参考文献
Schuurmans, Norbert; Uji-i, Hiroshi; Mamdouh, Wael; De Schryver, Frans C.; Feringa, Ben L.; Van Esch, Jan; De Feyter, Steven
Journal of the American Chemical Society, 2004 , vol. 126, # 43 p. 13884 - 13885
Schuurmans, Norbert; Uji-i, Hiroshi; Mamdouh, Wael; De Schryver, Frans C.; Feringa, Ben L.; Van Esch, Jan; De Feyter, Steven
Journal of the American Chemical Society, 2004 , vol. 126, # 43 p. 13884 - 13885
Schuurmans, Norbert; Uji-i, Hiroshi; Mamdouh, Wael; De Schryver, Frans C.; Feringa, Ben L.; Van Esch, Jan; De Feyter, Steven
Journal of the American Chemical Society, 2004 , vol. 126, # 43 p. 13884 - 13885