4-(乙基氨基)苯甲醛(9ci)合成路线 （共 14 条）
反应条件
potassium hydroxide in ethanol Heating;
参考文献
Bahner,C.T. et al.
Journal of Medicinal Chemistry, 1965 , vol. 8, p. 390 - 392
反应条件
sodium carbonate in water
T=130°C; 15 h; Autoclave;
参考文献
Wang, Bingshuai; Yu, Fabiao; Li, Peng; Sun, Xiaofei; Han, Keli
Dyes and Pigments, 2013 , vol. 96, # 2 p. 383 - 390
反应条件
hydrogenchloride; monoethylamine hydrochloride
1) sealed tube, 150 grad C, 40 h, 2) aq. HCl, room temp.; Yield given. Multistep reaction;
参考文献
Yudin, L. G.; Blokhin, A. V.; Bundel', Yu. G.; Simkin, B. Ya.; Terenin, V. I.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 11 p. 2064 - 2068
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 11 p. 2361 - 2366
反应条件
1: 80 percent / H2O / 10 h / Ambient temperature
2: 1) C2H5NH2*HCl, 2) aq. HCl / 1) sealed tube, 150 grad C, 40 h, 2) aq. HCl, room temp.
View Scheme
参考文献
Yudin, L. G.; Blokhin, A. V.; Bundel', Yu. G.; Simkin, B. Ya.; Terenin, V. I.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 11 p. 2064 - 2068
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 11 p. 2361 - 2366
反应条件
1: 1.) K2CO3 / 1.) acetone, 30 min, 2.) acetone, reflux, 4 h
2: 65 percent / KOH / toluene / 4 h / Heating
View Scheme
参考文献
Goswami; Borthakur; Rastogi
Journal of Chemical Research - Part S, 1996 , # 9 p. 424 - 425
反应条件
formaldehyd; 4-hydroxyl-amino-toluene-sulfonic acid-(2)
man zersetzt das Reaktionsprodukt durch Kochen mit Ammoniak;
参考文献
Geigy and Co.
Patent: DE103578 ;
Full Text Show Details
Geigy and Co.
Patent: DE105105 ;
参考文献
Yudin, L. G.; Blokhin, A. V.; Terenin, V. I.; Bundel', Yu. G.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, # 2 p. 406
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 2 p. 462
反应条件
hydrogenchloride; potassium dichromate
man fuegt eine salzsaure, mit Formaldehyd versetzte Loesung von Aethylanilin hinzu; Kochen des Kondensationsprodukts mit Mineralsaeure;
参考文献
Walter
Patent: DE118567 ;
参考文献
Yudin, L. G.; Blokhin, A. V.; Simkin, B. Ya.; Terenin, V. I.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 1598
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 8 p. 1785 - 1786
反应条件
1: Heating
2: HCl
View Scheme
参考文献
Yudin, L. G.; Blokhin, A. V.; Simkin, B. Ya.; Terenin, V. I.
Journal of Organic Chemistry USSR (English Translation), 1981 , vol. 17, p. 1598
Zhurnal Organicheskoi Khimii, 1981 , vol. 17, # 8 p. 1785 - 1786
