5-甲氧基-2-苯基-1H-苯并咪唑合成路线 (共 21 条)
反应条件
sodium dithionite in methanol
T=70°C; 0.6 h;
参考文献
Zhou, Binhua; Li, Baojian; Yi, Wei; Bu, Xianzhang; Ma, Lin
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 13 p. 3759 - 3763
反应条件
carbon monoxide; 1,10-phenanthroline monohydrate; bis(dibenzylideneacetone)-palladium(0) in N,N-dimethyl-formamide
T=120°C; P=4560.31 Torr; 193.75 h;
参考文献
Hubbard, Jeremiah W.; Piegols, Adam M.; Soederberg, Bjoern C.G.
Tetrahedron, 2007 , vol. 63, # 30 p. 7077 - 7085
反应条件
air in 1,4-dioxane
T=100°C; 6 h;
参考文献
Lin, Songnian; Yang, Lihu
Tetrahedron Letters, 2005 , vol. 46, # 25 p. 4315 - 4319
反应条件
2,6-dimethylpyridine; bis(triphenylphosphine)palladium(II)-chloride in N,N-dimethyl acetamide
T=140°C; P=4912.9 Torr; 24 h;
参考文献
Perry; Wilson
Journal of Organic Chemistry, 1993 , vol. 58, # 25 p. 7016 - 7021
反应条件
indium; acetic acid in ethyl acetate
0.5 h; RefluxInert atmosphere;
参考文献
Kim, Jaeho; Kim, Jihye; Lee, Hyunseung; Lee, Byung Min; Kim, Byeong Hyo
Tetrahedron, 2011 , vol. 67, # 41 p. 8027 - 8033
反应条件
N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran
T=50°C; 15 h; Inert atmosphere;
参考文献
Yamamoto, Yuhei; Mizuno, Hiroo; Tsuritani, Takayuki; Mase, Toshiaki
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1394 - 1396
反应条件
triphenyl phosphite in pyridine
T=220°C; 0.166667 h; microwave irradiation;
参考文献
Lin, Shou-Yuan; Isome, Yuko; Stewart, Ethan; Liu, Ji-Feng; Yohannes, Daniel; Yu, Libing
Tetrahedron Letters, 2006 , vol. 47, # 17 p. 2883 - 2886
反应条件
TEA; p-methylbenzenesulfonyl (tosylate) in chloroform
T=-20 - 20°C; 3 h;
参考文献
Yamamoto, Yuhei; Tsuritani, Takayuki; Mase, Toshiaki
Tetrahedron Letters, 2008 , vol. 49, # 5 p. 876 - 878
反应条件
copper(I) oxide; potassium carbonate; N-methyl-2-(methylamino)ethylamine in water
T=100°C; 30 h; Sealed tube;
参考文献
Peng, Jinsong; Ye, Min; Zong, Cuijuan; Hu, Fangyun; Feng, Lingtong; Wang, Xiaoyan; Wang, Yufeng; Chen, Chunxia
Journal of Organic Chemistry, 2011 , vol. 76, # 2 p. 716 - 719
反应条件
potassium carbonate in water
T=100°C; 30 h; Schlenk techniqueGreen chemistry;
参考文献
Chen, Chunxia; Chen, Chen; Li, Bin; Tao, Jingwei; Peng, Jinsong
Molecules, 2012 , vol. 17, # 11 p. 12506 - 12520