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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
79887-20-0
合成路线
(共 6 条)
125151-58-8
→
反应条件
79887-20-0
反应条件
potassium hydroxide; isopropyl alcohol Heating;
参考文献
Vasconcelos, Ursula B.; Schrader, Abel; Vilela, Guilherme D.; Borges, Antonio C.A.; Merlo, Aloir A.
Tetrahedron, 2008 , vol. 64, # 20 p. 4619 - 4626
116223-57-5
+
1066-54-2
三甲基乙炔基硅
→
反应条件
79887-20-0
反应条件
1: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide in triethylamine 2: With potassium carbonate in methanol 6 h;
参考文献
Lydon, Donocadh P.; Porres, Laurent; Beeby, Andrew; Marder, Todd B.; Low, Paul J.
New Journal of Chemistry, 2005 , vol. 29, # 7 p. 972 - 976
693-58-3
1-溴壬烷
→
反应条件
79887-20-0
反应条件
1: KOH / ethanol; H2O 2: triphenylphosphine; triethylamine / bis(triphenylphosphine) palladium dichloride; copper(I) iodide / tetrahydrofuran / 2 h / Heating 3: KOH / toluene / Heating View Scheme
参考文献
Yang; Tang; Gong; Wen
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2000 , vol. 348, p. 153 - 165
540-38-5
4-碘苯酚
→
反应条件
79887-20-0
反应条件
1: KOH / ethanol; H2O 2: triphenylphosphine; triethylamine / bis(triphenylphosphine) palladium dichloride; copper(I) iodide / tetrahydrofuran / 2 h / Heating 3: KOH / toluene / Heating View Scheme
参考文献
Yang; Tang; Gong; Wen
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2000 , vol. 348, p. 153 - 165
116223-57-5
→
反应条件
79887-20-0
反应条件
1: triphenylphosphine; triethylamine / bis(triphenylphosphine) palladium dichloride; copper(I) iodide / tetrahydrofuran / 2 h / Heating 2: KOH / toluene / Heating View Scheme
参考文献
Yang; Tang; Gong; Wen
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, 2000 , vol. 348, p. 153 - 165
105100-90-1
→
反应条件
79887-20-0
反应条件
1: copper(I)iodide, triphenylphosphine / dichlorobis(triphenylphosphine)palladium / triethylamine / 90 °C 2: sodium hydride / toluene; paraffin / 110 °C View Scheme
参考文献
Seto; Shimojitosho; Imazaki; Matsubara; Takahashi
Bulletin of the Chemical Society of Japan, 1990 , vol. 63, # 4 p. 1020 - 1025