(9CI)-2-亚硝基-嘧啶合成路线 (共 4 条)
反应条件
manganese(IV) oxide in chloroform
T=20°C; 0.166667 h;
参考文献
Moskalenko, G. G.; Sedova, V. F.; Mamaev, V. P.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1989 , vol. 25, # 7 p. 805 - 811
Khimiya Geterotsiklicheskikh Soedinenii, 1989 , vol. 25, # 7 p. 962 - 968
反应条件
dimethylsulfide; 3-chloro-benzenecarboperoxoic acid in dichloromethane
T=-7 - 20°C; 0.75 h;
参考文献
Taylor, Edward C.; Tseng, Chi-Ping; Rampal, Jang B.
Journal of Organic Chemistry, 1982 , vol. 47, # 3 p. 552 - 555
反应条件
1: S,S-dimethyl-N-(2-pyrimidinyl)sulfilimine With m-CBPO in dichloromethane
T=0°C; Inert atmosphere;
2: dimethylsulfide in dichloromethane
Inert atmosphere;
参考文献
Yang, Baiyuan; Zoellner, Tina; Gebhardt, Peter; Moellmann, Ute; Miller, Marvin J.
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 3 p. 691 - 697
反应条件
in sulfolane; methanol; dichloromethane; water
参考文献
The Regents of the University of California
Patent: US5843943 A1, 1998 ;
US 5843943 A