3-(3-苯基哌啶-3-基)丙酸甲酯合成路线 （共 7 条）
反应条件
1: CH2Cl2 / 7 h / Ambient temperature
2: NaBH4 / ethanol / 1.) 0 deg C, 1 h, 2.) room temperature, 4 h
View Scheme
参考文献
Buchanan, George L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2669 - 2670
反应条件
2: 2) Borch reduction
View Scheme
参考文献
Buchanan, Geo L.
Journal of the Chemical Society, Chemical Communications, 1981 , # 15 p. 814 - 815
反应条件
2: CH2Cl2 / 7 h / Ambient temperature
3: NaBH4 / ethanol / 1.) 0 deg C, 1 h, 2.) room temperature, 4 h
View Scheme
参考文献
Buchanan, George L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2669 - 2670
反应条件
1: 8.38 g / 6M HCl / 5 h / Heating
2: 90 percent / 0.58 h / 230 °C
4: CH2Cl2 / 7 h / Ambient temperature
5: NaBH4 / ethanol / 1.) 0 deg C, 1 h, 2.) room temperature, 4 h
View Scheme
参考文献
Buchanan, George L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2669 - 2670
反应条件
W-4 Raney nickel in benzene
8 h; Heating;
参考文献
Buchanan, George L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2669 - 2670
反应条件
2) Borch reduction; Multistep reaction;
参考文献
Buchanan, Geo L.
Journal of the Chemical Society, Chemical Communications, 1981 , # 15 p. 814 - 815
反应条件
hydrogenchloride
7 h; Heating;
参考文献
Buchanan, George L.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 11 p. 2669 - 2670
