1-(3-((6-氯-2-甲氧基-9-吖啶基)氨基)丙基)-5-甲基-2,4(1H,3H)-嘧啶二酮合成路线 （共 4 条）
反应条件
potassium carbonate in dimethyl sulfoxide
48 h; Ambient temperature;
参考文献
Bolte; Demuynck; Lhomme; et al.
Journal of the American Chemical Society, 1982 , vol. 104, # 3 p. 760 - 765
反应条件
in various solvent(s)
T=120°C; 2 h;
参考文献
Bolte; Demuynck; Lhomme; et al.
Journal of the American Chemical Society, 1982 , vol. 104, # 3 p. 760 - 765
反应条件
1: 30 percent / 47percent hydrobromic acid, sulfuric acid / 4 h / 70 °C
2: 75 percent / anhydrous potassium carbonate / dimethylsulfoxide / 48 h / Ambient temperature
View Scheme
参考文献
Bolte; Demuynck; Lhomme; et al.
Journal of the American Chemical Society, 1982 , vol. 104, # 3 p. 760 - 765
反应条件
1: 90 percent / dimethylsulfoxide / 12 h / 110 °C
2: 30 percent / 47percent hydrobromic acid, sulfuric acid / 4 h / 70 °C
3: 75 percent / anhydrous potassium carbonate / dimethylsulfoxide / 48 h / Ambient temperature
View Scheme
参考文献
Bolte; Demuynck; Lhomme; et al.
Journal of the American Chemical Society, 1982 , vol. 104, # 3 p. 760 - 765
