N'-(2-氯乙基)-N-(2-(甲基磺酰基)乙基)-N'-亚硝基脲合成路线 （共 3 条）
反应条件
dihydrogen peroxide in acetone
T=0°C; 1 h;
参考文献
Madelmont, J. C.; Godeneche, D.; Parry, D.; Duprat, J.; Chabard, J. L.; et al.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 9 p. 1346 - 1350
反应条件
1: sodium nitrite / formic acid; H2O / 1 h / 0 °C
2: 70 percent / H2O2 / formic acid / 0.17 h / 0 - 40 °C
View Scheme
参考文献
Madelmont, J. C.; Godeneche, D.; Parry, D.; Duprat, J.; Chabard, J. L.; et al.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 9 p. 1346 - 1350
反应条件
dihydrogen peroxide; sodium nitrite
1.) formic acid, H2O, 0 deg C, 1 h, 2.) formic acid, from 0 to 40 deg C, 10 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Madelmont, J. C.; Godeneche, D.; Parry, D.; Duprat, J.; Chabard, J. L.; et al.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 9 p. 1346 - 1350
