反应条件
1.1: 90 percent / aq. p-toluenesulfonic acid / methanol / 79 °C
2.1: 14.7 g / aq. NaIO4 / tetrahydrofuran / 22 h / 20 °C
3.1: MgSO4 / tetrahydrofuran
3.2: 90 percent / LiAlH4 / tetrahydrofuran
4.1: BBr3 / CH2Cl2 / 3 h / 20 °C
5.1: NaH / tetrahydrofuran / 0.17 h / 20 °C
5.2: 3.22 g / tetrahydrofuran / 4.5 h
View Scheme
参考文献
Huang, Audris; Kodanko, Jeremy J.; Overman, Larry E.
Journal of the American Chemical Society, 2004 , vol. 126, # 43 p. 14043 - 14053
