C6H5MgBr; C2H5OH; pyridine in diethyl ether (C6H5)2SiCl2 and C6H5MgBr in ether; addn. of C2H5OH and pyridine;;
参考文献
Freiser, H.; Eagle, M. V.; Speier, J.
Journal of the American Chemical Society, 1953 , vol. 75, p. 2824 - 2827
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Gmelin Handbook: Si: MVol.C, 76, page 212 - 214
in tetrahydrofuran mixing at -78°C for 0.5 h; warming to room temp.;; aq. NH4Cl was added; organic layer was sepd., evapd., crystd. from CH2Cl2-petroleum ether; elem. anal.;;
参考文献
Adams, Stefan; Draeger, Martin
Journal of Organometallic Chemistry, 1987 , vol. 323, p. 11 - 20
