N-甲基-N-亚硝基对甲苯磺酰胺合成路线 (共 111 条)
反应条件
potassium hydroxide in tetrahydrofuran; methanol; water T=20°C; Arndt-Eistert Homologation;
参考文献
Organic Letters, , vol. 15, # 21 p. 5590 - 5593
反应条件
potassium hydroxide in ethanol T=5 - 10°C; 3 h; Yields of byproduct given;
参考文献
Polivka, Zdenek; Metys, Jan; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 9 p. 2034 - 2049
反应条件
potassium hydroxide in ethanol T=5 - 10°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Polivka, Zdenek; Metys, Jan; Protiva, Miroslav
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 9 p. 2034 - 2049
反应条件
potassium hydroxide in tetrahydrofuran; methanol; water T=20°C;
参考文献
Mastronardi, Federica; Gutmann, Bernhard; Oliver Kappe
Organic Letters, 2013 , vol. 15, # 21 p. 5590 - 5593
反应条件
in 1,4-dioxane; water T=25°C; solvent isotope effect (kH/kD); Rate constant;
参考文献
Garcia-Rio, Luis; Iglesias, Emilia; Leis, J. Ramon; Pena, M. Elena; Rios, Ana
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 1 p. 29 - 37
反应条件
1: N-methyl-N-nitroso-p-toluene-sulphonamide With potassium hydroxide in diethyl ether; ethanol; water 2: 3,4-dihydroxy-3-cyclobutene-1,2-dione in diethyl ether; ethanol; water T=20°C;
参考文献
Miles, D.Howard; Payne, Matthew
Tetrahedron, 2001 , vol. 57, # 27 p. 5769 - 5772
反应条件
in 1,4-dioxane; sodium hydroxide T=25°C; var. acidity; Rate constant;
参考文献
Leis, J. Ramon; Rios, Ana
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1996 , # 5 p. 857 - 864
反应条件
in 1,4-dioxane; sodium hydroxide T=25°C; other phenols; var. dioxane conc. and acidity; Product distributionMechanism;
参考文献
Leis, J. Ramon; Rios, Ana
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1996 , # 5 p. 857 - 864
反应条件
N-hexadecyl-N,N,N-trimethylammonium bromide in ethanol T=25°C;
参考文献
Castro, Albino; Leis, J. Ramon; Pena, M. Elena
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1990 , # 7 p. 1221 - 1225
反应条件
potassium hydroxide in methanol; water T=20°C; 1.16667 h;
参考文献
Pinho, Vagner D.; Gutmann, Bernhard; Miranda, Leandro S. M.; De Souza, Rodrigo O. M. A.; Kappe, C. Oliver
Journal of Organic Chemistry, 2014 , vol. 79, # 4 p. 1555 - 1562