4-甲基-N-(2-甲基苯基)苯磺酰胺合成路线 （共 22 条）
反应条件
1: silica gel 2: tris-(dibenzylideneacetone)dipalladium(0); potassium phosphate; di-tert-butyl(2′,4′,6′-triisopropylbiphenyl-2-yl)phosphine / 1,1-dimethylpropan-1-ol / 15 h / 80 °C / Inert atmosphere View Scheme
参考文献
Journal of Organic Chemistry, , vol. 76, # 11 p. 4552 - 4563
反应条件
1: potassium carbonate / acetonitrile 2: tris-(dibenzylideneacetone)dipalladium(0); potassium phosphate; di-tert-butyl(2′,4′,6′-triisopropylbiphenyl-2-yl)phosphine / 1,1-dimethylpropan-1-ol / 15 h / 80 °C / Inert atmosphere View Scheme
参考文献
Journal of Organic Chemistry, , vol. 76, # 11 p. 4552 - 4563
反应条件
1.1: pyridine / 0.5 h / 20 - 100 °C / |Inert atmosphere 2.1: magnesium / diethyl ether / 0.17 h / |Inert atmosphere; |Reflux 2.2: 0.5 h / |Inert atmosphere; |Heating 3.1: FeCl3·6H2O / 4 h / 60 °C / |Inert atmosphere View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 45, # 1 p. 28 - 43
反应条件
1.1: magnesium / diethyl ether / 0.17 h / |Inert atmosphere; |Reflux 1.2: 0.5 h / |Inert atmosphere; |Heating 2.1: FeCl3·6H2O / 4 h / 60 °C / |Inert atmosphere View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 45, # 1 p. 28 - 43
反应条件
1.1: acetic acid / 15 h / |Inert atmosphere; |Reflux 2.1: pyridine / 0.5 h / 20 - 100 °C / |Inert atmosphere 3.1: magnesium / diethyl ether / 0.17 h / |Inert atmosphere; |Reflux 3.2: 0.5 h / |Inert atmosphere; |Heating 4.1: FeCl3·6H2O / 4 h / 60 °C / |Inert atmosphere View Scheme
参考文献
Organic Preparations and Procedures International, , vol. 45, # 1 p. 28 - 43
反应条件
1: glacial acetic acid; nitric acid 2: sulfuric acid View Scheme
参考文献
Am.Cyanamid Co.
Patent: US2459002 , 1944 ;
反应条件
bei hoeherer Temperatur erhaelt man ein Gemisch von Nitrierungsprodukten.Hydrolysis;
参考文献
Morgan; Challenor
Journal of the Chemical Society, 1921 , vol. 119, p. 1540
反应条件
water; nitric acid
Erhitzen des Reaktionsprodukts mit konz.Schwefelsaeure;
参考文献
Platt; Sharp
Journal of the Chemical Society, 1948 , p. 2129,2132
反应条件
bei hoeherer Temperatur erhaelt man ein Gemisch von Nitrierungsprodukten.Hydrolysis;
参考文献
Morgan; Challenor
Journal of the Chemical Society, 1921 , vol. 119, p. 1540
反应条件
sulfuric acid; sodium nitrite in acetic acid
1 h;
参考文献
Zakatov, V. V.; Dubina, V. L.; Gladshtein, I. Ya.
Journal of Organic Chemistry USSR (English Translation), 1986 , vol. 22, p. 540 - 542
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 3 p. 604 - 606
