1,3-二甲基-2-咪唑啉酮合成路线 (共 79 条)
反应条件
sodium methylate in methanol
反应条件
phosgene in toluene T=0 - 40°C;
参考文献
Herres-Pawlis, Sonja; Floerke, Ulrich; Henkel, Gerald
European Journal of Inorganic Chemistry, 2005 , # 19 p. 3815 - 3824
反应条件
in toluene T=20 - 60°C; 14 h;
参考文献
Raab, Volker; Harms, Klaus; Sundermeyer, Joerg; Kovacevic, Borislav; Maksic, Zvonimir B.
Journal of Organic Chemistry, 2003 , vol. 68, # 23 p. 8790 - 8797
反应条件
in 1,2-dichloro-ethane T=70°C; 3 h;
参考文献
Hamed, Atef; Mueller, Edgar; Jochims, Johannes C.
Tetrahedron, 1986 , vol. 42, # 24 p. 6645 - 6656
反应条件
sodium methylate in methanol
参考文献
Yoshimitsu, Takehiko; Arano, Yoshimasa; Nagaoka, Hiroto
Journal of the American Chemical Society, 2005 , vol. 127, # 33 p. 11610 - 11611
参考文献
YAMANOUCHI PHARMACEUTICAL CO. LTD.; Helix Research Institute
Patent: EP1213353 A1, 2002 ;
反应条件
sodium hydroxide in water T=25°C; hydrolytic decomposition; Rate constant;
参考文献
Kankaanperae, Alpo; Scharlin, Pirketta; Kuusisto, Ilona; Kallio, Riitta; Bernoulli, Emma
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 2 p. 169 - 174
反应条件
sodium hydroxide in water T=25°C; hydrolytic decomposition; Rate constant;
参考文献
Kankaanperae, Alpo; Scharlin, Pirketta; Kuusisto, Ilona; Kallio, Riitta; Bernoulli, Emma
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 2 p. 169 - 174