N-({3-氯-4-[(4-氯苄基)磺酰基]苯基}氨基甲酰)-2,6-二氟苯甲酰胺合成路线 （共 30 条）
反应条件
The reaction was carried out via isothiouronium salt.;
参考文献
Doyama, Kazuo; Hama, Fumio; Sakata, Yoshiteru; Misumi, Soichi
Tetrahedron Letters, 1981 , vol. 22, # 41 p. 4101 - 4104
参考文献
Meij, Paul F. C. van der; Pandit, Upendra K.
Tetrahedron Letters, 1988 , vol. 29, # 42 p. 5445 - 5448
反应条件
triethylamine in ethanol
参考文献
Doyama, Kazuo; Hama, Fumio; Sakata, Yoshiteru; Misumi, Soichi
Tetrahedron Letters, 1981 , vol. 22, # 41 p. 4101 - 4104
反应条件
1: 83 percent / triethylamine / ethanol
2: 28 percent / potassium carbonate / dimethylsulfoxide / dilution condition
View Scheme
参考文献
Doyama, Kazuo; Hama, Fumio; Sakata, Yoshiteru; Misumi, Soichi
Tetrahedron Letters, 1981 , vol. 22, # 41 p. 4101 - 4104
反应条件
triethylamine in ethanol
参考文献
Doyama, Kazuo; Hama, Fumio; Sakata, Yoshiteru; Misumi, Soichi
Tetrahedron Letters, 1981 , vol. 22, # 41 p. 4101 - 4104
反应条件
1: The reaction was carried out via isothiouronium salt.
2: 83 percent / triethylamine / ethanol
View Scheme
参考文献
Doyama, Kazuo; Hama, Fumio; Sakata, Yoshiteru; Misumi, Soichi
Tetrahedron Letters, 1981 , vol. 22, # 41 p. 4101 - 4104
反应条件
sodium hydroxide; thiourea
1.) ethanol, reflux, 8 h; 2.) water, 90 deg C, 10 min; 1 h, heating; Yield given. Multistep reaction;
参考文献
Doyama, Kazuo; Higashii, Takayuki; Seyama, Fumio; Sakata, Yoshiteru; Misumi, Soichi
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 3619 - 3628
反应条件
potassium carbonate in dimethyl sulfoxide
dilution condition;
参考文献
Doyama, Kazuo; Higashii, Takayuki; Seyama, Fumio; Sakata, Yoshiteru; Misumi, Soichi
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 3619 - 3628
反应条件
sodium hydride in N,N-dimethyl-formamide
参考文献
Doyama, Kazuo; Higashii, Takayuki; Seyama, Fumio; Sakata, Yoshiteru; Misumi, Soichi
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 3619 - 3628
反应条件
potassium carbonate in dimethyl sulfoxide
dilution condition;
参考文献
Doyama, Kazuo; Higashii, Takayuki; Seyama, Fumio; Sakata, Yoshiteru; Misumi, Soichi
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 3619 - 3628
