2-乙烯基-4H-1,3-二噻英合成路线 （共 12 条）
反应条件
in chloroform-d1
T=25°C; 144 h;
参考文献
Block,E.; Ahmad,S.; Cataflamo,J.L.
Journal of the American Chemical Society, 1986 , vol. 108, p. 7045
反应条件
hydrogen sulfide; orthoformic acid triethyl ester; zinc(II) chloride in ethanol
T=0°C; 2.5 h; Yield given. Yields of byproduct given;
参考文献
Beslin, Pierre
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1753 - 1754
反应条件
in dichloromethane
T=28°C; Irradiation;
参考文献
Vedejs, E.; Eberlein, T. H.; Varie, D. L.
Journal of the American Chemical Society, 1982 , vol. 104, # 5 p. 1445 - 1447
反应条件
Bis(dimethylaluminium)sulfid in tetrahydrofuran; toluene
T=65°C; Dimerization; substitution; Diels-Alder reaction; 4.5 h; Title compound not separated from byproducts.;
参考文献
Li, Guang Ming; Niu, Shuqiang; Segi, Masahito; Tanaka, Koichiro; Nakajima, Tadashi; Zingaro, Ralph A.; Reibenspies, Joseph H.; Hall, Michael B.
Journal of Organic Chemistry, 2000 , vol. 65, # 20 p. 6601 - 6612
反应条件
Bis(dimethylaluminium)sulfid in tetrahydrofuran; toluene
T=65°C; Cycloaddition; substitution; Diels-Alder reaction; 4.5 h;
参考文献
Li, Guang Ming; Niu, Shuqiang; Segi, Masahito; Tanaka, Koichiro; Nakajima, Tadashi; Zingaro, Ralph A.; Reibenspies, Joseph H.; Hall, Michael B.
Journal of Organic Chemistry, 2000 , vol. 65, # 20 p. 6601 - 6612
参考文献
Bock, Hans; Mohmand, Shamsher; Hirabayashi, Takakuni; Semkow, Andrzej
Journal of the American Chemical Society, 1982 , vol. 104, # 1 p. 312 - 313
反应条件
cobalt(II) chloride in acetonitrile
T=20°C; Title compound not separated from byproducts;
参考文献
Capperucci, Antonella; Degl'Innocenti, Alessandro; Biondi, Simona; Nocentini, Tiziano; Rinaudo, Giuseppe
Tetrahedron Letters, 2003 , vol. 44, # 14 p. 2831 - 2835
反应条件
T=50°C; 168 h; Further byproducts given;
参考文献
Block,E.; Iyer,R.; Grisoni,S.
Journal of the American Chemical Society, 1988 , vol. 110, p. 7813
反应条件
T=506.9°C; P=1 Torr; Yield given. Yields of byproduct given;
参考文献
Bock, Hans; Mohmand, Shamsher; Hirabayashi, Takakuni; Semkow, Andrzej
Chemische Berichte, 1982 , vol. 115, # 4 p. 1339 - 1348
反应条件
T=37°C; 48 h; other temperatures, other times; Product distribution;
参考文献
Block; Ahmad; Jain; et al.
Journal of the American Chemical Society, 1984 , vol. 106, # 26 p. 8295 - 8296
