N-乙基-2-溴苯甲酰胺合成路线 (共 14 条)
反应条件
1,4-diaza-bicyclo[2.2.2]octane; copper(l) iodide; 1,10-phenanthroline; tetra-(n-butyl)ammonium iodide in water
T=20 - 160°C; 48.5 h; Inert atmosphere;
参考文献
Wang, Fei; Chen, Chao; Deng, Geng; Xi, Chanjuan
Journal of Organic Chemistry, 2012 , vol. 77, # 8 p. 4148 - 4151
反应条件
tert.-butyl lithium in diethyl ether
0.5 h; Yields of byproduct given;
参考文献
Beak, Peter; Musick, Timothy J.; Liu, Chao; Cooper, Thomas; Gallagher, Donald J.
Journal of Organic Chemistry, 1993 , vol. <26> 58, p. 7330 - 7335
反应条件
CuPF6(MeCN)2; caesium carbonate in toluene
Heatingother reagents; Product distribution;
参考文献
Kalinin, Alexey V.; Bower, Justin F.; Riebel, Peter; Snieckus, Victor
Journal of Organic Chemistry, 1999 , vol. 64, # 9 p. 2986 - 2987
反应条件
tert.-butyl lithium in tetrahydrofuran
T=-78°C; 0.5 h; other base, solvent; Product distribution;
参考文献
Beak, Peter; Musick, Timothy J.; Liu, Chao; Cooper, Thomas; Gallagher, Donald J.
Journal of Organic Chemistry, 1993 , vol. <26> 58, p. 7330 - 7335