苄基2-脱氧-2-邻苯二甲酰亚胺基-3,4,6-三-O-乙酰基-beta-D-吡喃葡萄糖苷合成路线 （共 5 条）
反应条件
1: H2NNH2*H2O / ethanol / 18 h / Heating 2: pyridine / 21 h / 20 °C 3: 72 percent / potassium tert-butanolate / methanol; tetrahydrofuran / 4 h View Scheme
参考文献
Kamst, Eric; Zegelaar-Jaarsveld, Korien; Van Der Marel, Gijs A.; Van Boom, Jacques H.; Lugtenberg, Ben J.J.; Spaink, Herman P.
Carbohydrate Research, 1999 , vol. 321, # 3-4 p. 176 - 189
反应条件
1: H2NNH2*H2O / ethanol / 18 h / Heating 2: pyridine / 21 h / 20 °C View Scheme
参考文献
Carbohydrate Research, , vol. 321, # 3-4 p. 176 - 189
反应条件
1: H2NNH2*H2O / ethanol / 18 h / Heating 2: pyridine / 21 h / 20 °C 3: 72 percent / potassium tert-butanolate / methanol; tetrahydrofuran / 4 h View Scheme
参考文献
Kamst, Eric; Zegelaar-Jaarsveld, Korien; Van Der Marel, Gijs A.; Van Boom, Jacques H.; Lugtenberg, Ben J.J.; Spaink, Herman P.
Carbohydrate Research, 1999 , vol. 321, # 3-4 p. 176 - 189
反应条件
With sodium methylate in methanol T=0°C;
参考文献
Charon; Szabo Carbohydrate research, 1983 , vol. 111, # 2 p. C13-15
反应条件
Multi-step reaction with 2 steps 1: 92 percent / conc. HCl / acetone / 70 °C2: 82 percent / TsOH / dimethylformamide / 50 °C
参考文献
Wang, Lai-Xi; Li, Chuan; Wang, Qin-Wei; Hui, Yong-Zheng Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1994 , # 6 p. 621 - 628
