苄基2-脱氧-2-邻苯二甲酰亚胺基-beta-D-吡喃葡萄糖苷合成路线 （共 4 条）
反应条件
With sodium methylate in methanol T=0°C;
参考文献
Charon; Szabo Carbohydrate research, 1983 , vol. 111, # 2 p. C13-15
反应条件
Multi-step reaction with 2 steps 1: 79.3 percent / mercury(II) cyanide / nitromethane; toluene / 20 °C / 4 Angstroem molecular sieve2: 90.2 percent / sodium methoxide / methanol / 4 h
参考文献
Charon, Daniel; Mondange, Michelle; Szabo, Ladislas Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 10 p. 2291 - 2296
反应条件
Multi-step reaction with 2 steps 1: 88 percent / silver trifluoromethanesulfonate, 2,4,6-trimethylpyridine / nitromethane / 2 h / -30 °C2: 97 percent / conc. hydrochloric acid / H2O; acetone / 6 h / 70 °C
参考文献
Lemieux, R. U.; Abbas, S. Z.; Chung, B. Y. Canadian Journal of Chemistry, 1982 , vol. 60, p. 58 - 62
反应条件
Multi-step reaction with 2 steps 1.1: boron trifluoride diethyl etherate / dichloromethane / 24 h / 20 °C / |Inert atmosphere2.1: sodium methylate / methanol / -10 °C / |Inert atmosphere2.2: Amberlite ion exchange resin / pH 7
参考文献
Wasonga, Gilbert; Tatara, Yota; Kakizaki, Ikuko; Huang, Xuefei Journal of Carbohydrate Chemistry, 2013 , vol. 32, # 5-6 p. 392 - 409
