2-氨基-4-苯基苯甲酸甲酯合成路线 （共 5 条）
反应条件
palladium hydroxide on carbon; hydrogen in methanol
P=760.051 Torr; 16 h;
参考文献
Stammers, Timothy A.; Coulombe, Rene; Rancourt, Jean; Thavonekham, Bounkham; Fazal, Gulrez; Goulet, Sylvie; Jakalian, Araz; Wernic, Dominic; Tsantrizos, Youla; Poupart, Marc-Andre; Boes, Michael; McKercher, Ginette; Thauvette, Louise; Kukolj, George; Beaulieu, Pierre L.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 9 p. 2585 - 2589
反应条件
acetic acid in methanol; hexane; ethyl acetate
参考文献
TOYAMA CHEMICAL CO., LTD.
Patent: EP1820795 A1, 2007 ;
EP 1820795 A1
反应条件
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / water; ethylene glycol dimethyl ether / 20 h / 80 °C
2: diethyl ether
3: palladium hydroxide on carbon; hydrogen / methanol / 16 h / 760.05 Torr
View Scheme
参考文献
Stammers, Timothy A.; Coulombe, Rene; Rancourt, Jean; Thavonekham, Bounkham; Fazal, Gulrez; Goulet, Sylvie; Jakalian, Araz; Wernic, Dominic; Tsantrizos, Youla; Poupart, Marc-Andre; Boes, Michael; McKercher, Ginette; Thauvette, Louise; Kukolj, George; Beaulieu, Pierre L.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 9 p. 2585 - 2589
反应条件
1: sodium carbonate; tetrakis(triphenylphosphine) palladium(0) / water; ethylene glycol dimethyl ether / 20 h / 80 °C
2: diethyl ether
3: palladium hydroxide on carbon; hydrogen / methanol / 16 h / 760.05 Torr
View Scheme
参考文献
Stammers, Timothy A.; Coulombe, Rene; Rancourt, Jean; Thavonekham, Bounkham; Fazal, Gulrez; Goulet, Sylvie; Jakalian, Araz; Wernic, Dominic; Tsantrizos, Youla; Poupart, Marc-Andre; Boes, Michael; McKercher, Ginette; Thauvette, Louise; Kukolj, George; Beaulieu, Pierre L.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 9 p. 2585 - 2589
反应条件
1: diethyl ether
2: palladium hydroxide on carbon; hydrogen / methanol / 16 h / 760.05 Torr
View Scheme
参考文献
Stammers, Timothy A.; Coulombe, Rene; Rancourt, Jean; Thavonekham, Bounkham; Fazal, Gulrez; Goulet, Sylvie; Jakalian, Araz; Wernic, Dominic; Tsantrizos, Youla; Poupart, Marc-Andre; Boes, Michael; McKercher, Ginette; Thauvette, Louise; Kukolj, George; Beaulieu, Pierre L.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 9 p. 2585 - 2589
