2-甲基-3,4'-联吡啶-6(1H)-酮合成路线 （共 7 条）
反应条件
1: 82 percent / N-bromosuccinimide / methanol / 5 h / Ambient temperature 2: 62 percent / 18-crown-6 / acetonitrile / 120 h / Heating View Scheme
参考文献
Shiao, Min-Jen; Shyu, Li-Ming; Chen, Chieh-Fu
Heterocycles, 1990 , vol. 31, # 3 p. 523 - 527
反应条件
hydrogen; palladium on activated charcoal in methanol
2 h;
参考文献
Shiao, Min-Jen; Shyu, Li-Ming; Chen, Chieh-Fu
Heterocycles, 1990 , vol. 31, # 3 p. 523 - 527
反应条件
sulfur in various solvent(s)
T=195 - 200°C; 4.5 h;
参考文献
Singh, Baldev
Synthesis, 1985 , # 3 p. 305 - 306
反应条件
hydrogen bromide in methanol
50 h; Heating;
参考文献
Shiao, Min-Jen; Shyu, Li-Ming; Chen, Chieh-Fu
Heterocycles, 1990 , vol. 31, # 3 p. 523 - 527
反应条件
1: tetrahydrofuran / 0.5 h / -25 °C
3: 82 percent / 48percent HBr / methanol / 50 h / Heating
View Scheme
参考文献
Shiao, Min-Jen; Shyu, Li-Ming; Chen, Chieh-Fu
Heterocycles, 1990 , vol. 31, # 3 p. 523 - 527
反应条件
2: 82 percent / 48percent HBr / methanol / 50 h / Heating
View Scheme
参考文献
Shiao, Min-Jen; Shyu, Li-Ming; Chen, Chieh-Fu
Heterocycles, 1990 , vol. 31, # 3 p. 523 - 527
反应条件
1: 46 percent / t-C4H9OK / dioxane / 1.) room temp., 40 min., 2.) 1.5 h
2: 83 percent / S8 / various solvent(s) / 4.5 h / 195 - 200 °C
View Scheme
参考文献
Singh, Baldev
Synthesis, 1985 , # 3 p. 305 - 306
