(E,E)-2,6-二甲基-2,6-辛二烯二醛合成路线 (共 9 条)
反应条件
manganese(IV) oxide in chloroform
48 h;
参考文献
Dawson, Glenn W.; Pickett, John A.; Smiley, Diane W. M.
Bioorganic and Medicinal Chemistry, 1996 , vol. 4, # 3 p. 351 - 361
反应条件
pyridinium chlorochromate in dichloromethane
3 h; Ambient temperature;
参考文献
Veith, Martin; Dettner, Konrad; Boland, Wilhelm
Tetrahedron, 1996 , vol. 52, # 19 p. 6601 - 6612
反应条件
selenium(IV) oxide in dichloromethane
T=25°C; Title compound not separated from byproducts.;
参考文献
Santangelo; Rotticci; Liblikas; Norin; Unelius
Journal of Organic Chemistry, 2001 , vol. 66, # 16 p. 5384 - 5387
反应条件
1: 40 percent / SeO2, t-BuOOH / toluene / 120 h / Ambient temperature
2: 87 percent / aq. K2CO3 / methanol / 1 h
3: 88 percent / MnO2 / CHCl3 / 48 h
View Scheme
参考文献
Dawson, Glenn W.; Pickett, John A.; Smiley, Diane W. M.
Bioorganic and Medicinal Chemistry, 1996 , vol. 4, # 3 p. 351 - 361
反应条件
1: 87 percent / aq. K2CO3 / methanol / 1 h
2: 88 percent / MnO2 / CHCl3 / 48 h
View Scheme
参考文献
Dawson, Glenn W.; Pickett, John A.; Smiley, Diane W. M.
Bioorganic and Medicinal Chemistry, 1996 , vol. 4, # 3 p. 351 - 361
反应条件
1: 41 percent / KBH4, LiCl, Amberlit IR C-50 / propan-2-ol; dioxane / 10 h / 20 °C
2: MnO2 / CHCl3 / 60 h
View Scheme
参考文献
Battersby, Alan R.; Thompson, Mervyn; Gluesenkamp, Karl-Heinz; Tietze, Lutz-F.
Chemische Berichte, 1981 , vol. 114, # 10 p. 3430 - 3438
反应条件
manganese(IV) oxide in chloroform
60 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Battersby, Alan R.; Thompson, Mervyn; Gluesenkamp, Karl-Heinz; Tietze, Lutz-F.
Chemische Berichte, 1981 , vol. 114, # 10 p. 3430 - 3438
反应条件
selenium(IV) oxide in ethanol
0.75 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Battersby, Alan R.; Thompson, Mervyn; Gluesenkamp, Karl-Heinz; Tietze, Lutz-F.
Chemische Berichte, 1981 , vol. 114, # 10 p. 3430 - 3438
反应条件
nicotinamide adenine dinucleotide
Rauwolfia serpentina cell suspension cultures, pH 6.5, incubation;
参考文献
Uesato; Ikeda; Fujita; et al.
Tetrahedron Letters, 1987 , vol. 28, # 38 p. 4431 - 4434