4-溴-2,6-二异丙基苯胺合成路线 （共 4 条）
反应条件
N-bromosuccinmide in N,N-dimethyl-formamide T=0 - 5°C; 0.333333 h; Inert atmosphere;
参考文献
UNIVERSAL DISPLAY CORPORATION; XIA, Chuanjin; YEAGER, Walter; LI, David Zenan; FIORDELISIO, James; MA, Bin; ELSHENAWY, Zeinab; LAYEK, Suman; BARRON, Edward; KOTTAS, Gregg; BROOKS, Jason
Patent: WO2012/116231 A2, 2012 ;
Location in patent: Page/Page column 120 ;
反应条件
bromine in methanol; acetic acid 2 h;
参考文献
Liu, Hua-Rong; Gomes, Pedro T.; Costa, Sandra I.; Duarte, M. Teresa; Branquinho; Fernandes, Anabela C.; Chien, James C.W.; Singh; Marques, Maria M.
Journal of Organometallic Chemistry, 2005 , vol. 690, # 5 p. 1314 - 1323
反应条件
1-methyl-1H-imidazole; potassium carbonate; copper(l) chloride in o-xylene T=140°C; 30 h; Inert atmosphereSchlenk technique;
参考文献
Organic Process Research and Development, , vol. 12, # 3 p. 537 - 539
反应条件
hydrogenchloride; hypophosphorous ether; sodium nitrite
T=4 - 20°C; Inert atmosphere;
参考文献
Coombs, John R.; Haeffner, Fredrik; Kliman, Laura T.; Morken, James P.
Journal of the American Chemical Society, 2013 , vol. 135, # 30 p. 11222 - 11231
