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乙二醇
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63148-62-9
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二甲基亚砜
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
80065-55-0
合成路线
（共 11 条）
98-17-9
3-三氟甲基苯酚
→
反应条件
80065-55-0
反应条件
1: 69 percent / KOH / 2-ethoxy-ethanol / 8 h / Heating 2: 75 percent / H2 / Raney Ni / ethanol; dioxane / 1.25 h / 2327.2 Torr 3: 57 percent / Et3N / 2-ethoxy-ethanol / 6.5 h / 105 °C 4: hydrazine hydrate / ethanol / 6 h / Heating View Scheme
参考文献
LaMontagne, Maurice P.; Blumbergs, Peter; Strube, Richard E.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 9 p. 1094 - 1097
82333-37-7
→
反应条件
80065-55-0
反应条件
1: 75 percent / H2 / Raney Ni / ethanol; dioxane / 1.25 h / 2327.2 Torr 2: 57 percent / Et3N / 2-ethoxy-ethanol / 6.5 h / 105 °C 3: hydrazine hydrate / ethanol / 6 h / Heating View Scheme
参考文献
LaMontagne, Maurice P.; Blumbergs, Peter; Strube, Richard E.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 9 p. 1094 - 1097
81358-81-8
→
反应条件
80065-55-0
反应条件
1: 69 percent / POCl3 / 2 h / 80 °C 2: 69 percent / KOH / 2-ethoxy-ethanol / 8 h / Heating 3: 75 percent / H2 / Raney Ni / ethanol; dioxane / 1.25 h / 2327.2 Torr 4: 57 percent / Et3N / 2-ethoxy-ethanol / 6.5 h / 105 °C 5: hydrazine hydrate / ethanol / 6 h / Heating View Scheme
参考文献
LaMontagne, Maurice P.; Blumbergs, Peter; Strube, Richard E.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 9 p. 1094 - 1097
81358-92-1
→
反应条件
80065-55-0
反应条件
1: 69 percent / KOH / 2-ethoxy-ethanol / 8 h / Heating 2: 75 percent / H2 / Raney Ni / ethanol; dioxane / 1.25 h / 2327.2 Torr 3: 57 percent / Et3N / 2-ethoxy-ethanol / 6.5 h / 105 °C 4: hydrazine hydrate / ethanol / 6 h / Heating View Scheme
参考文献
LaMontagne, Maurice P.; Blumbergs, Peter; Strube, Richard E.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 9 p. 1094 - 1097
64992-96-7
→
反应条件
80065-55-0
反应条件
1: 92 percent / conc. HCl / ethanol / 21 h / Heating 2: 69 percent / POCl3 / 2 h / 80 °C 3: 69 percent / KOH / 2-ethoxy-ethanol / 8 h / Heating 4: 75 percent / H2 / Raney Ni / ethanol; dioxane / 1.25 h / 2327.2 Torr 5: 57 percent / Et3N / 2-ethoxy-ethanol / 6.5 h / 105 °C 6: hydrazine hydrate / ethanol / 6 h / Heating View Scheme
参考文献
LaMontagne, Maurice P.; Blumbergs, Peter; Strube, Richard E.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 9 p. 1094 - 1097
82333-46-8
→
反应条件
80065-55-0
反应条件
hydrazine hydrate in ethanol 6 h; Heating;
参考文献
LaMontagne, Maurice P.; Blumbergs, Peter; Strube, Richard E.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 9 p. 1094 - 1097
82333-41-3
→
反应条件
80065-55-0
反应条件
1: 57 percent / Et3N / 2-ethoxy-ethanol / 6.5 h / 105 °C 2: hydrazine hydrate / ethanol / 6 h / Heating View Scheme
参考文献
LaMontagne, Maurice P.; Blumbergs, Peter; Strube, Richard E.
Journal of Medicinal Chemistry, 1982 , vol. 25, # 9 p. 1094 - 1097
98081-50-6
→
反应条件
80065-55-0
反应条件
1: hydrogenchloride; water / ethanol / Reflux 2: phosphoric acid / 100 °C 3: 10 palladium on activated charcoal; hydrazine hydrate / ethanol / Reflux 4: sodium tetrahydroborate; acetic acid / 20 °C 5: hydrazine hydrate / ethanol / Reflux View Scheme
参考文献
Chaurasiya, Narayan D.; Ganesan, Shobana; Nanayakkara, N.P. Dhammika; Dias, Luiza R.S.; Walker, Larry A.; Tekwani, Babu L.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 4 p. 1701 - 1704
1061346-40-4
→
反应条件
80065-55-0
反应条件
1: phosphoric acid / 100 °C 2: 10 palladium on activated charcoal; hydrazine hydrate / ethanol / Reflux 3: sodium tetrahydroborate; acetic acid / 20 °C 4: hydrazine hydrate / ethanol / Reflux View Scheme
参考文献
Chaurasiya, Narayan D.; Ganesan, Shobana; Nanayakkara, N.P. Dhammika; Dias, Luiza R.S.; Walker, Larry A.; Tekwani, Babu L.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 4 p. 1701 - 1704
160088-53-9
→
反应条件
80065-55-0
反应条件
1: potassium hydroxide / N,N-dimethyl-formamide / 100 °C 2: hydrogenchloride; water / ethanol / Reflux 3: phosphoric acid / 100 °C 4: 10 palladium on activated charcoal; hydrazine hydrate / ethanol / Reflux 5: sodium tetrahydroborate; acetic acid / 20 °C 6: hydrazine hydrate / ethanol / Reflux View Scheme
参考文献
Chaurasiya, Narayan D.; Ganesan, Shobana; Nanayakkara, N.P. Dhammika; Dias, Luiza R.S.; Walker, Larry A.; Tekwani, Babu L.
Bioorganic and Medicinal Chemistry Letters, 2012 , vol. 22, # 4 p. 1701 - 1704
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