(6-溴-吡啶-2-基)-苯甲酮合成路线 （共 4 条）
反应条件
1: 2,5-dibromo-pyridine With n-butyllithium in diethyl ether; hexane
T=-75°C; 0.5 h;
2: N,N-dimethyl benzamide in diethyl ether; hexane
0.583333 h;
参考文献
Gracel Display Inc.
Patent: US2009/62542 A1, 2009 ;
Location in patent: Page/Page column 11-12 ;
反应条件
1: 6-BrNA With thionyl chloride
3 h; Reflux;
2: benzene With AlCl3, aluminium chloride
T=5°C; Reflux;
参考文献
MERCK SHARP and DOHME CORP.; DANG, Qun; ZHOU, Changyou; ZOU, Wuxin; HUA, Yuxia
Patent: WO2013/43624 A1, 2013 ;
Location in patent: Page/Page column 45 ;
反应条件
AlCl3, aluminium chloride
6 h; Reflux;
参考文献
MERCK SHARP and DOHME CORP.; ZHOU, Changyou; ZOU, Wuxin; HUA, Yuxia; DANG, Qun
Patent: WO2013/40790 A1, 2013 ;
Location in patent: Page/Page column 45 ;
反应条件
1: thionyl chloride / 3 h / |Reflux
2: AlCl3, aluminium chloride / 6 h / |Reflux
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参考文献
MERCK SHARP and DOHME CORP.; ZHOU, Changyou; ZOU, Wuxin; HUA, Yuxia; DANG, Qun
Patent: WO2013/40790 A1, 2013 ;
