2,5-二甲基苯甲酰基甲酸乙酯合成路线 （共 3 条）
反应条件
aluminium trichloride in chloroform
T=0 - 5°C; 1.33333 h;
参考文献
Itoh, Osamu; Nagata, Takayoshi; Nomura, Isamu; Takanaga, Tetsuya; Sugita, Toshio; Ichikawa, Katsuhiko
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 810 - 814
反应条件
1: 1,4-dimethyl-2-chlorobenzene With lithium in diethyl ether
T=3 - 6°C;
2: With copper (I) cyanide in tetrahydrofuran; diethyl ether
T=-80 - -25°C; 0.416667 h;
3: oxalic acid monoethyl ester chloride in tetrahydrofuran; diethyl ether
T=-80°C;
参考文献
Screttas, Constantinos G.; Steele, Barry R.; Micha-Screttas, Maria; Heropoulos, Georgios A.
Organic Letters, 2012 , vol. 14, # 22 p. 5680 - 5683
反应条件
aluminium trichloride in chloroform
T=0 - 5°C; 1.33333 h; modification without solvent (other time);
参考文献
Itoh, Osamu; Nagata, Takayoshi; Nomura, Isamu; Takanaga, Tetsuya; Sugita, Toshio; Ichikawa, Katsuhiko
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 810 - 814
