3-(2-硝基苯基)-2-丙炔-1-醇合成路线 （共 5 条）
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in benzene
T=60°C; 0.333333 h;
参考文献
Ozeki, Minoru; Muroyama, Atsushi; Kajimoto, Tetsuya; Watanabe, Tetsushi; Wakabayashi, Keiji; Node, Manabu
Synlett, 2009 , # 11 p. 1781 - 1784
反应条件
copper(l) iodide; triethylamine; bis-triphenylphosphine-palladium(II) chloride
T=20°C;
参考文献
Yin, Yan; Ma, Wenying; Chai, Zhuo; Zhao, Gang
Journal of Organic Chemistry, 2007 , vol. 72, # 15 p. 5731 - 5736
反应条件
sodium hydroxide; water in acetone
Combinatorial reaction / High throughput screening (HTS);
参考文献
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE; UNIVERSITE DE RENNES 1
Patent: US2007/43234 A1, 2007 ;
Location in patent: Page/Page column 58 ;
反应条件
1: copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); triethylamine / 2 h / 20 °C / Inert atmosphere
2: ethanol; pyridinium p-toluenesulfonate / 20 °C
View Scheme
参考文献
Maji, Manasi; Mallick, Dibyendu; Mondal, Sayantan; Anoop, Anakuthil; Bag, Subhendu Sekhar; Basak, Amit; Jemmis, Eluvathingal D.
Organic Letters, 2011 , vol. 13, # 5 p. 888 - 891
反应条件
manganese(IV) oxide; potassium hydroxide in benzene
T=20°C; 0.333333 h;
参考文献
Bumagin, N. A.; Ponomarev, A. B.; Beletskaya, I. P.
Doklady Chemistry, 1985 , vol. 283, p. 212 - 214
Dokl. Akad. Nauk SSSR Ser. Khim., 1985 , vol. 283, # 3 p. 630 - 633
