反应条件
Stage #1: <a href="#" onclick="return RXDsubstances(event, this, '2045666', constants.ctx, '0')">p-trifluoromethylphenyl bromide</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '1209227', constants.ctx, '0')">n-butyllithium</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1696894', constants.ctx, '0')">diethyl ether</a>; <a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a> <br />T=-78 - 0°C; 1 h; <br />Stage #2: <a href="#" onclick="return RXDsubstances(event, this, '1779789', constants.ctx, '0')">ethyl Pentafluoropropionate</a> <b>With</b> <a href="#" onclick="return RXDsubstances(event, this, '2349612', constants.ctx, '0')">boron trifluoride diethyl etherate</a> <b>in</b> <a href="#" onclick="return RXDsubstances(event, this, '1696894', constants.ctx, '0')">diethyl ether</a>; <a href="#" onclick="return RXDsubstances(event, this, '1730733', constants.ctx, '0')">hexane</a> <br />T=-78°C; 3 h; <br />
参考文献
Davies, Alyn T.; Slawin, Alexandra M. Z.; Smith, Andrew D. Chemistry - A European Journal, 2015 , vol. 21, # 52 p. 18944 - 18948