802294-64-0合成路线 （共 916 条）
反应条件
hydrazine hydrate 3 h; Heating;
参考文献
Basanagouda, Mahantesha; Kulkarni, Manohar V.; Kalkhambkar, Raj G.; Kulkarni, Geeta M.
Synthetic Communications, 2008 , vol. 38, # 17 p. 2929 - 2940
反应条件
Amberlyst 15 T=120°C; Friedel-Crafts acylation; 24 h;
参考文献
Baisch, Gabi; Wagner, Barbara; Oehrlein, Reinhold
Tetrahedron, 2010 , vol. 66, # 21 p. 3742 - 3748
反应条件
in acetonitrile Electrolysis; 6.5 h, initial voltage 40 V; mixture was filtered, solvent removed at 60°C in vacuo, solids were collected, washed with diethyl ether, dried at 110°C; elem.anal.;
参考文献
Kumar, N.; Tuck, Dennis G.; Watson, Katherine D.
Canadian Journal of Chemistry, 1987 , vol. 65, p. 740 - 743
反应条件
in water stirring (reflux, 6 h); filtration, washing (Et2O), evapn. of the aq. phase to dryness, grounding in a pestle and mortar, drying in vacuo over P2O5, drying in vacuo at 160°C for 4 h; elem. anal.;
参考文献
Hulme, Charlotte E.; Watkinson, Michael; Haynes, Michaela; Pritchard, Robin G.; McAuliffe, Charles A.; et al.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1997 , # 11 p. 1805 - 1814
反应条件
propionic anhydride in propionic acid byproducts: acetic acid; dissolution of acetate in EtCOOH, distn. of acetic acid, addn. of propionic anhydride, refluxing (30 min.); removal of EtCOOH (distn.), acetone addn., pptn., filtration, drying (vac.); elem. anal.;
参考文献
Hasenkox, Ulrich; Mitze, Carsten; Waser, Rainer
Journal of the American Ceramic Society, 1997 , vol. 80, # 10 p. 2709 - 2713
反应条件
sodium hydroxide in not given pptn. with NaOH, washing the ppt., treating with organic acid;
参考文献
Vlase; Chiriac; Doca
Journal of Thermal Analysis and Calorimetry, 2003 , vol. 72, # 3 p. 839 - 845
反应条件
hydrogen sulfide; triethylamine; isobutyl chloroformate in dichloromethane T=-10°C; 1.) 40 min; 1 h;
参考文献
Fujimoto; Iwano; Hirai; Sugawara
Chemical and Pharmaceutical Bulletin, 1986 , vol. 34, # 3 p. 999 - 1014
反应条件
T=160 - 200°C; unter Abdestillieren des gebildeten Wassers;
参考文献
Seeliger,W.; Thier,W.
Justus Liebigs Annalen der Chemie, 1966 , vol. 698, p. 158 - 166
反应条件
dicyclohexyl-carbodiimide in dichloromethane
参考文献
Ke, Damei; Zhan, Chuanlang; Li, Xiao; Li, Alexander D.Q.; Yao, Jiannian
Tetrahedron, 2009 , vol. 65, # 39 p. 8269 - 8276
反应条件
scandium tris(trifluoromethanesulfonate) in toluene T=129°C;
参考文献
Novus International Inc.
Patent: US2007/292485 A1, 2007 ;
Location in patent: Page/Page column 15 ;
