802294-64-0合成路线 (共 916 条)
反应条件
T=100 - 150°C; Dean-StarkInert atmosphere;
参考文献
Duris, Andrej; Barber, David M.; Sanganee, Hitesh J.; Dixon, Darren J.
Chemical Communications, 2013 , vol. 49, # 27 p. 2777 - 2779
反应条件
T=20 - 145°C; 3.33 h; Inert atmosphere;
参考文献
Garcia, Pierre; Harrak, Youssef; Diab, Lisa; Cordier, Pierre; Ollivier, Cyril; Gandon, Vincent; Malacria, Max; Fensterbank, Louis; Aubert, Corinne
Organic Letters, 2011 , vol. 13, # 11 p. 2952 - 2955
反应条件
tert.-butylhydroperoxide; sulfuric acid 7.7 h;
参考文献
Richardson, William H.; Thomson, Stephen A.
Journal of Organic Chemistry, 1982 , vol. 47, # 23 p. 4515 - 4520
反应条件
sodium tetrahydroborate 1.) benzene, RT, 45 min, 2.) benzene, reflux, 5.5 h; Multistep reaction;
参考文献
Cannon, Joseph G.; Perez, Julio A.; Pease, Jonathan P; Long, John Paul; Flynn, Jan R.; et al.
Journal of Medicinal Chemistry, 1980 , vol. 23, # 7 p. 745 - 749
反应条件
boron trifluoride T=150°C; unter Druck;
参考文献
Kindler; Oelschlaeger
Chemische Berichte, 1954 , vol. 87, p. 194,201
参考文献
Tsatsas; Delaby
Annales Pharmaceutiques Francaises, 1956 , vol. 14, p. 621,634
参考文献
Pickard; Kenyon
Journal of the Chemical Society, 1913 , vol. 103, p. 1940,1935
Journal of the Chemical Society, 1911 , vol. 99, p. 55,64
反应条件
ammonia; metasilicic acid T=500°C;
参考文献
Celanese Corp.Am.
Patent: US2590986 , 1950 ;
参考文献
Sowa; Nieuwland
Journal of the American Chemical Society, 1937 , vol. 59, p. 1203
反应条件
1: propionic acid in dichloromethane T=0°C; 0.25 h; 2: 1,2-diamino-benzene With pyridine in dichloromethane T=20°C; 6 h; Further stages.;
参考文献
Kaul, Savita; Kumar, Ajay; Sain, Bir; Bhatnagar
Synthetic Communications, 2007 , vol. 37, # 15 p. 2457 - 2460