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乙二醇
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63148-62-9
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丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
80231-53-4
合成路线
(共 5 条)
68236-21-5
2-氯-7-甲基-3-喹啉甲醛
→
反应条件
80231-53-4
反应条件
hydrazine hydrate in ethanol 0.5 h; Heating;
参考文献
Meth-Cohn, Otto; Narine, Bramha; Tarnowski, Brian; Hayes, Roy; Keyzad, Amitis; at al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2509 - 2517
80231-39-6
→
反应条件
80231-53-4
反应条件
1: 87 percent / toluene-p-sulphonic acid / benzene / Heating 2: 87 percent / BuLi, H2O / diethyl ether; hexane / -70 °C 3: 0.08 g / aq. HCl / diethyl ether; hexane 4: 84 percent / hydrazine hydrate / ethanol / 0.5 h / Heating View Scheme
参考文献
Meth-Cohn, Otto; Narine, Bramha; Tarnowski, Brian; Hayes, Roy; Keyzad, Amitis; at al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2509 - 2517
80231-43-2
→
反应条件
80231-53-4
反应条件
1: 87 percent / BuLi, H2O / diethyl ether; hexane / -70 °C 2: 0.08 g / aq. HCl / diethyl ether; hexane 3: 84 percent / hydrazine hydrate / ethanol / 0.5 h / Heating View Scheme
参考文献
Meth-Cohn, Otto; Narine, Bramha; Tarnowski, Brian; Hayes, Roy; Keyzad, Amitis; at al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2509 - 2517
80231-37-4
→
反应条件
80231-53-4
反应条件
1: 35 percent / Zn, aq. NaOH / ethanol / 120 h / Ambient temperature 2: 84 percent / hydrazine hydrate / ethanol / 0.5 h / Heating View Scheme
参考文献
Meth-Cohn, Otto; Narine, Bramha; Tarnowski, Brian; Hayes, Roy; Keyzad, Amitis; at al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2509 - 2517
80231-46-5
→
反应条件
80231-53-4
反应条件
1: 0.08 g / aq. HCl / diethyl ether / 1 h / Ambient temperature 2: 84 percent / hydrazine hydrate / ethanol / 0.5 h / Heating View Scheme
参考文献
Meth-Cohn, Otto; Narine, Bramha; Tarnowski, Brian; Hayes, Roy; Keyzad, Amitis; at al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 2509 - 2517