2-溴-1-[4-(2-甲基丙基)苯基]-1-丙酮合成路线 （共 13 条）
反应条件
perchloric acid; thallium(III) nitrate T=25°C; 30 h;
参考文献
Yamauchi, Takayoshi; Nakao, Kenji; Fujii, Kyoichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1255 - 1258
反应条件
methyloxirane in water; acetone IrradiationpH neutral;
参考文献
Sonawane, Harikisan; Bellur, Nanjundiah S.; Kulkarni, Dilip G.; Ayyangar, Nagaraj R.
Tetrahedron, 1994 , vol. 50, # 4 p. 1243 - 1260
反应条件
perchloric acid; thallium(III) nitrate T=25°C; 25 h;
参考文献
Yamauchi, Takayoshi; Nakao, Kenji; Fujii, Kyoichi
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1987 , p. 1255 - 1258
反应条件
methyloxirane in water; acetone IrradiationpH neutral;
参考文献
Tetrahedron, , vol. 50, # 4 p. 1243 - 1260
反应条件
methyloxirane in methanol IrradiationpH neutral;
参考文献
Sonawane, Harikisan; Bellur, Nanjundiah S.; Kulkarni, Dilip G.; Ayyangar, Nagaraj R.
Tetrahedron, 1994 , vol. 50, # 4 p. 1243 - 1260
反应条件
bromine in chloroform
参考文献
BLASCHIM S.p.A.
Patent: EP34871 B2, 1993 ;
反应条件
copper(ll) bromide in chloroform; ethyl acetate
2 h; Heating;
参考文献
Duh, Tsai-Hui; Wang, Yi-Fong; Wu, Ming-Jung
Journal of the Chinese Chemical Society (Taipei, Taiwan), 1995 , vol. 42, # 3 p. 579 - 584
参考文献
Syntex Pharmaceuticals International Limited
Patent: US4542237 A1, 1985 ;
反应条件
1: 85 percent / AlCl3 / 1,2-dichloro-ethane / 6 h / Ambient temperature
2: 1.) propylene oxide; 2.) NaOH / 1.) MeOH, irradiation, pH neutral; 2.) MeOH, reflux, 2 h
3: 85 percent / Br2 / CCl4 / 1 h
View Scheme
参考文献
Sonawane, Harikisan; Bellur, Nanjundiah S.; Kulkarni, Dilip G.; Ayyangar, Nagaraj R.
Tetrahedron, 1994 , vol. 50, # 4 p. 1243 - 1260
反应条件
1: 1.) propylene oxide; 2.) NaOH / 1.) MeOH, irradiation, pH neutral; 2.) MeOH, reflux, 2 h
2: 85 percent / Br2 / CCl4 / 1 h
View Scheme
参考文献
Sonawane, Harikisan; Bellur, Nanjundiah S.; Kulkarni, Dilip G.; Ayyangar, Nagaraj R.
Tetrahedron, 1994 , vol. 50, # 4 p. 1243 - 1260
